2-(2-chloroethyl)-malonaldehyde-1,3-dibenzenaminium chloride

Base Information

• Chemical Name: 2-(2-chloroethyl)-malonaldehyde-1,3-dibenzenaminium chloride
• CAS No.: 1293942-57-0
• Molecular Formula: C₁₇H₁₇ClN₂*ClH
• Molecular Weight: 321.249
• Mol file: 1293942-57-0.mol

Synonyms:

Chemical Property of 2-(2-chloroethyl)-malonaldehyde-1,3-dibenzenaminium chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-(2-chloroethyl)-malonaldehyde-1,3-dibenzenaminium chloride

There total 1 articles about 2-(2-chloroethyl)-malonaldehyde-1,3-dibenzenaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

4-butanolide (96-48-0) + aniline hydrochloride (142-04-1,36663-09-9) → 2-(2-chloroethyl)-malonaldehyde-1,3-dibenzenaminium chloride (1293942-57-0)

Guidance literature:

4-butanolide; With oxalyl dichloride; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; at 70 ℃; for 12h; Inert atmosphere;

aniline hydrochloride; With sodium hydrogencarbonate; In water; at 20 ℃; Inert atmosphere;

DOI:10.1021/ja1104014

upstream raw materials:

4-butanolide

aniline hydrochloride