C₂₀H₁₃NO₈

Base Information

• Chemical Name: C₂₀H₁₃NO₈
• CAS No.: 1314917-70-8
• Molecular Formula: C₂₀H₁₃NO₈
• Molecular Weight: 395.325
• Mol file: 1314917-70-8.mol

Synonyms:

Chemical Property of C₂₀H₁₃NO₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₁₃NO₈

There total 7 articles about C₂₀H₁₃NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H25NO11 (1314917-90-2) → C20H13NO8 (1314917-70-8)

Guidance literature:

With hydrogenchloride; In methanol;

DOI:10.1016/j.bmcl.2011.04.140

Reference yield:

1-hydroxy-3,6,7-tris(methoxymethoxy)-9H-xanthen-9-one (1314917-55-9) → C20H13NO8 (1314917-70-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 50 °C

2: hydrogenchloride / methanol

With hydrogenchloride; potassium carbonate; In methanol; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.04.140

Reference yield:

2,4,5-trimethoxybenzoyl chloride (42833-66-9) → C20H13NO8 (1314917-70-8)

Guidance literature:

Multi-step reaction with 6 steps

1: aluminum (III) chloride / diethyl ether / 48 h / 20 °C

2: pyridine; tetra(n-butyl)ammonium hydroxide / water / 4 h / Reflux

3: pyridine hydrochloride

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

5: potassium carbonate / N,N-dimethyl-formamide / 6 h / 50 °C

6: hydrogenchloride / methanol

With pyridine; hydrogenchloride; aluminum (III) chloride; tetra(n-butyl)ammonium hydroxide; pyridine hydrochloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 1: Friedel Crafts acylation;

DOI:10.1016/j.bmcl.2011.04.140

upstream raw materials:

C₂₆H₂₅NO₁₁

1-hydroxy-3,6,7-tris(methoxymethoxy)-9H-xanthen-9-one

2,4,5-trimethoxybenzoyl chloride

asaronic acid

Refernces