trans-[Pt(C₆F₅)Cl(P(C₆H₅)(CH₂)8CHCH(CH₂)8)2]

Base Information

Chemical Name:trans-[Pt(C₆F₅)Cl(P(C₆H₅)(CH₂)8CHCH(CH₂)8)2]
CAS No.:709008-43-5
Molecular Formula:C₅₄H₇₈ClF₅P₂Pt
Molecular Weight:1114.69
Hs Code.:

trans-[Pt(C<sub>6</sub>F<sub>5</sub>)Cl(P(C<sub>6</sub>H<sub>5</sub>)(CH<sub>2</sub>)8CHCH(CH<sub>2</sub>)8)2]

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Chemical Property of trans-[Pt(C₆F₅)Cl(P(C₆H₅)(CH₂)8CHCH(CH₂)8)2]

Chemical Property:

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Technology Process of trans-[Pt(C₆F₅)Cl(P(C₆H₅)(CH₂)8CHCH(CH₂)8)2]

There total 1 articles about trans-[Pt(C₆F₅)Cl(P(C₆H₅)(CH₂)8CHCH(CH₂)8)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 709008-35-5
trans-[Pt(C₆F₅)Cl(P(C₆H₅)((CH₂)8CHCH₂)2)2]

: 709008-43-5
trans-[Pt(C₆F₅)Cl(P(C₆H₅)(CH₂)8CHCH(CH₂)8)2]

Guidance literature:: Grubbs catalyst first generation; In dichloromethane; (N2); charging of two-necked flask with (Cl)(C6F5)Pt(PPh((CH2)8CHCH2)2)2, Grubbs' catalyst and CH2Cl2; reflux for 3.5 h; addn. of remaining catalyst, reflux for 3.5 h; removal of solvent by oil-pump vac., filtration through neutral alumina using CH2Cl2; removal of solvent from filtrate by oil-pump vac., elem. anal.;
DOI:10.1039/b400156g

Reference yield: 15.0%

: 709008-43-5
trans-[Pt(C₆F₅)Cl(P(C₆H₅)(CH₂)8CHCH(CH₂)8)2]

: 1333-74-0
hydrogen

: 709008-44-6
syn-trans-[Pt(C₆F₅)Cl(P(C₆H₅)(CH₂)18)2]

Guidance literature:: With Pd/C; In ethanol; 1,2-dichloro-ethane; (N2); charging of two-necked flask with (Z,Z)-trans-(Cl)(C6F5)Pt(PPh(CH2)8CHCH(CH2)8)2, Pd/C, ClCH2CH2Cl and ethanol; flushing with H2; fitting with a balloon of H2; stirring for 71 h; removal of solvent by oil-pump vac., filtration through neutral alumina using 3:1 v/v hexanes-CH2Cl2; removal of solvent from filtrate by oil-pump vac., as oil; elem. anal.;
DOI:10.1039/b400156g