ethyl (2-benzoyl-4-chlorophenyl)carbamate

Base Information

• Chemical Name: ethyl (2-benzoyl-4-chlorophenyl)carbamate
• CAS No.: 69565-58-8
• Molecular Formula: C29H17 Cr N4 O10 S . 2 Na
• Molecular Weight: 303.7403

Synonyms:1-Naphthalenesulfonicacid, 3-hydroxy-4-[(2-hydroxy-1-naphthalenyl)azo]-7-nitro-, chromium complex;Glycine, N-[(2-hydroxyphenyl)methylene]-, chromium complex

Chemical Property of ethyl (2-benzoyl-4-chlorophenyl)carbamate

Chemical Property:

• Vapor Pressure: 1.72E-07mmHg at 25°C
• Boiling Point: 426.8°C at 760 mmHg
• Flash Point: 211.9°C
• Density: 1.29g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl (2-benzoyl-4-chlorophenyl)carbamate

There total 2 articles about ethyl (2-benzoyl-4-chlorophenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

chloroformic acid ethyl ester (541-41-3) + 5-chloro-2-aminobenzophenone (719-59-5) → 2-Ethoxycarbonylamino-5-chlorbenzophenon (69565-58-8)

Guidance literature:

With pyridine; In chloroform; for 1h; Ambient temperature;

Reference yield:

→ 2-Ethoxycarbonylamino-5-chlorbenzophenon (69565-58-8)

Guidance literature:

Trichloracetamidbenzophenon 5, NH3, A.;

Reference yield: 82.0%

2-Ethoxycarbonylamino-5-chlorbenzophenon (69565-58-8) + 1-aminoguanidine hydrochloride (1937-19-5,16139-18-7) → C17H18ClN5O2*ClH (146470-03-3)

Guidance literature:

With hydrogenchloride; In ethanol; water; for 12h; Heating;

upstream raw materials:

chloroformic acid ethyl ester

5-chloro-2-aminobenzophenone

Downstream raw materials:

6-chloro-3-(3-morpholin-4-yl-propyl)-4-(3-morpholin-4-yl-propylamino)-4-phenyl-3,4-dihydro-1H-quinazolin-2-one

10-chloro-11b-phenyl-3,4,7,11b-tetrahydro-2H,6H<1,3>oxazino<3,2-c>quinazolin-6-one

C₁₇H₁₈ClN₅O₂*ClH

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