C₂₇H₂₄O₄

Base Information

Chemical Name:C₂₇H₂₄O₄
CAS No.:1427206-38-9
Molecular Formula:C₂₇H₂₄O₄
Molecular Weight:412.485
Hs Code.:

C<sub>27</sub>H<sub>24</sub>O<sub>4</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₄O₄

Chemical Property:

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Technology Process of C₂₇H₂₄O₄

There total 3 articles about C₂₇H₂₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 6-hydroxy-8-methoxy-3-methyl-1,2,3,4-tetrahydrotetraphene-7,12-dione

: 1427206-38-9
C₂₇H₂₄O₄

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1002/cjoc.201201084

Reference yield:

: 198132-48-8
ethyl (E,Z)-(+/-)-2-(3-methylcyclohexylidene)acetate

: 1427206-38-9
C₂₇H₂₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium; diisopropylamine; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 20 °C / Inert atmosphere

2.1: tetrahydrofuran; hexane / 0.08 h / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 2 h / Inert atmosphere

4.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; potassium carbonate; diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 2.1: |Diels-Alder Cycloaddition;
DOI:10.1002/cjoc.201201084

Reference yield:

: C₁₇H₃₂O₂Si

: 1427206-38-9
C₂₇H₂₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; hexane / 0.08 h / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 2 h / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 1: |Diels-Alder Cycloaddition;
DOI:10.1002/cjoc.201201084