trimesitylgermylisocyanate

Base Information

Chemical Name:trimesitylgermylisocyanate
CAS No.:145296-91-9
Molecular Formula:C₂₈H₃₃GeNO
Molecular Weight:472.166
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimesitylgermylisocyanate

Chemical Property:

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Technology Process of trimesitylgermylisocyanate

There total 2 articles about trimesitylgermylisocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 62120-68-7
chlorotri(2,4,6-trimethylphenyl)germane

: 3315-16-0
silver cyanate

: 145296-91-9
trimesitylgermylisocyanate

Guidance literature:: In tetrahydrofuran; byproducts: AgCl; addn. of the Ge compd. in THF to AgNCO in THF (inert gas) and stirring at 20°C for 40 h; decantation, evapn. and recrystn. from ether at -20°C;

Reference yield: 35.0%

: 139925-54-5
trimesitylgermylamine

: 145296-91-9
trimesitylgermylisocyanate

: 23932-77-6
trimesitylgermyl hydroxide

Guidance literature:: With carbon dioxide; In benzene; bubbling of dry CO2 through a soln. of the Ge compd. in benzene (inert gas) and heating in a sealed tube at 66°C for 24 h; identification by gas chromy., IR and NMR;