Germane, chlorotris(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:Germane, chlorotris(2,4,6-trimethylphenyl)-
CAS No.:62120-68-7
Molecular Formula:C27H33ClGe
Molecular Weight:465.602
Hs Code.:
DSSTox Substance ID:DTXSID30456798
Nikkaji Number:J636.237K
Wikidata:Q82279372

Synonyms:Germane, chlorotris(2,4,6-trimethylphenyl)-;Trimesitylchlorogermane;62120-68-7;DTXSID30456798

Suppliers and Price of Germane, chlorotris(2,4,6-trimethylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germane, chlorotris(2,4,6-trimethylphenyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:466.1482565
Heavy Atom Count:29
Complexity:437

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)[Ge](C2=C(C=C(C=C2C)C)C)(C3=C(C=C(C=C3C)C)C)Cl)C

Technology Process of Germane, chlorotris(2,4,6-trimethylphenyl)-

There total 13 articles about Germane, chlorotris(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 139925-54-5
trimesitylgermylamine

: 62120-68-7
chlorotri(2,4,6-trimethylphenyl)germane

Guidance literature:: With aq. HCl; In benzene; byproducts: NH4Cl; 20°C, 5 h;
DOI:10.1016/0022-328X(92)83032-D

Reference yield: 88.0%

: 3265-03-0
trimesitylgermane

: 62120-68-7
chlorotri(2,4,6-trimethylphenyl)germane

Guidance literature:: With tetrachloromethane; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; byproducts: CHCl3; a soln. of Ge-compound in CCl4 was heated at 90°C for 2 h in thepresence of AIBN; evapd., recrystd. from n-pentane; elem. anal.;
DOI:10.1016/S0022-328X(00)81378-9

Reference yield: 80.0%

: 120154-50-9
trimesitylgermyllithium

: 24973-59-9
2,4,6-tri-tert-butyl-1-nitrosobenzene

: 3265-03-0
trimesitylgermane

: 62120-68-7
chlorotri(2,4,6-trimethylphenyl)germane

: 2816-43-5
triphenylgermane

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; diethyl ether; inert atmosphere; addn. of org. compd. soln. (THF) to soln. of Ge-compd. (THF/Et2O) at -20°C, keeping at same temp. for 30 min, at room temp. for 1 h, soln. hydrolysis; twice extn. (Et2O), drying (Na2SO4), soln. concn. (reduced pressure); (1)H-NMR and ESR spectroscopy;
DOI:10.1016/0022-328X(93)80008-Y