Technology Process of 1,1,1-Tris(2,4,6-trimethylphenyl)germanamine
There total 3 articles about 1,1,1-Tris(2,4,6-trimethylphenyl)germanamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
tetrahydrofuran; hexane;
byproducts: LiCl; addn. of n-BuLi in hexane to dry NH3 in abs. THF at -30°C (inert gas), addn. of the Ge compd. in THF at room temp.; stored at 20°C for 48 h; evapn., addn. of benzene, filtn. (LiCl) and evapn.;
- Guidance literature:
-
In
diethyl ether;
byproducts: NaCl; addn. of the Ge compd. in abs. ether to NaNH2 in ether (inert gas), cooling to -80°C and addn. of dry NH3, warmimg to room temp. (within 20 h); addn. of abs. benzene, filtn. and evapn. (vac.); elem. anal.;
