C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3

Base Information

Chemical Name:C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3
CAS No.:349658-50-0
Molecular Formula:C₃₅H₂₉Fe₂O₂P
Molecular Weight:624.282
Hs Code.:

C<sub>5</sub>H<sub>5</sub>FeC<sub>5</sub>H<sub>4</sub>C<sub>5</sub>H<sub>5</sub>Fe(CO)2P(C<sub>6</sub>H<sub>5</sub>)3

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Suppliers and Price of C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3

Chemical Property:

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Technology Process of C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3

There total 3 articles about C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.8%

: 12078-28-3,38979-86-1
dicarbonylcyclopentadienyliodoiron(II)

: tri-n-butylstannylferrocene

: 603-35-0
triphenylphosphine

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 349658-57-7
C₅H₅FeC₅H₄COFe(C₅H₅)(CO)P(C₆H₅)3

: 349658-50-0
C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3

Guidance literature:: With C₄H₉Li; In tetrahydrofuran; hexane; byproducts: (C4H9)4Sn, ferrocene, LiI; (N2); addn. of a soln. of BuLi in hexane to a soln. of iron complex in THF at-78°C, stirring for 30 min, addn. to a mixt. of phosphine with iron iodide complex in THF at -78°C, stirring overnight; addn. of water, extn. with Et2O, drying (MgSO4), evapn., column chromy (SiO2, ethyl acetate/hexane 1:10), evapn.; elem. anal;
DOI:10.1021/om0008528

Reference yield: 22.0%

: 12078-28-3,38979-86-1
dicarbonylcyclopentadienyliodoiron(II)

: 349658-73-7
C₅H₄Sn(C₄H₉)3FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3

: 603-35-0
triphenylphosphine

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 349658-50-0
C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3

: (C₅H₄C₅H₅Fe(CO)2P(C₆H₅)3)Fe(C₅H₄COFe(C₅H₅)(CO)P(C₆H₅)3)

: 349658-66-8
[Fe([μ,η5:η4-5-exo-(1'-C5H4)C5H5]Fe(CO)2PPh3)2]

Guidance literature:: With C₄H₉Li; In tetrahydrofuran; hexane; byproducts: (C4H9)4Sn, LiI; (N2); addn. of a soln. of BuLi in hexane to a soln. of iron complex in THF at -78°C, stirring for 1 h, addn. to a mixt of phosphine and iron iodide complex in THF at -78°C, warming to room temp., stirring overnight; addn. of water, extn. with Et2O, drying (MgSO4), evapn., column chromy (SiO2, ethyl acetate/hexane 1:9), evapn.;
DOI:10.1021/om0008528

Reference yield: 13.0%

: 12078-28-3,38979-86-1
dicarbonylcyclopentadienyliodoiron(II)

: 1,1'-dilithioferrocene N,N,N'N'-tetramethylethylenediamine

: 603-35-0
triphenylphosphine

: 349658-57-7
C₅H₅FeC₅H₄COFe(C₅H₅)(CO)P(C₆H₅)3

: 349658-50-0
C₅H₅FeC₅H₄C₅H₅Fe(CO)2P(C₆H₅)3

: (C₅H₄COFe(C₅H₅)(CO)P(C₆H₅)3)2Fe

: (C₅H₄C₅H₅Fe(CO)2P(C₆H₅)3)Fe(C₅H₄COFe(C₅H₅)(CO)P(C₆H₅)3)

: 349658-66-8
[Fe([μ,η5:η4-5-exo-(1'-C5H4)C5H5]Fe(CO)2PPh3)2]

Guidance literature:: In tetrahydrofuran; byproducts: [C5H5Fe(CO)2]2, ferrocene, LiI; (N2); addn. of a soln. of iron lithium complex in THF to a soln. of ironiodide complex and phosphine in THF at -78°C, warming to room te mp., stirring overnight; addn. of water, extn. with Et2O, drying (MgSO4), evapn., column chromy (SiO2, ethyl acetate/hexane 1:10-1:3), evapn.; elem. anal;
DOI:10.1021/om0008528