C₂₈H₁₈F₃N

Base Information

Chemical Name:C₂₈H₁₈F₃N
CAS No.:1309688-98-9
Molecular Formula:C₂₈H₁₈F₃N
Molecular Weight:425.453
Hs Code.:

C<sub>28</sub>H<sub>18</sub>F<sub>3</sub>N

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₁₈F₃N

Chemical Property:

Purity/Quality:

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Technology Process of C₂₈H₁₈F₃N

There total 5 articles about C₂₈H₁₈F₃N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1309688-76-3
C₂₈H₁₄F₅NO₂

: 128796-39-4
4-trifluoromethylphenylboronic acid

: 1309688-98-9
C₂₈H₁₈F₃N

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; In acetonitrile; for 6h; Reflux;
DOI:10.1055/s-0030-1259556

Reference yield:

: 512787-24-5
2-benzoylphenyl trifluoromethanesulfonate

: 1309688-98-9
C₂₈H₁₈F₃N

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; triethylamine / N,N-dimethyl-formamide / 2.5 h / 70 °C

2: pyridine; hydroxylamine hydrochloride / 2.5 h / 100 °C

3: triethylamine / dichloromethane / 0.5 h / 0 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / acetonitrile / 6 h / Reflux

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydroxylamine hydrochloride; tetrabutylammomium bromide; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1055/s-0030-1259556

Reference yield:

: 117-99-7
2-Hydroxybenzophenone

: 1309688-98-9
C₂₈H₁₈F₃N

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine; dmap / dichloromethane / 1.5 h / -78 - 0 °C

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; triethylamine / N,N-dimethyl-formamide / 2.5 h / 70 °C

3: pyridine; hydroxylamine hydrochloride / 2.5 h / 100 °C

4: triethylamine / dichloromethane / 0.5 h / 0 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / acetonitrile / 6 h / Reflux

With pyridine; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydroxylamine hydrochloride; tetrabutylammomium bromide; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1055/s-0030-1259556