Technology Process of C48H54N2O4
There total 8 articles about C48H54N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 90 percent / nitric acid, conc. sulfuric acid / 0.5 h / 75 °C
2: p-methoxyphenylthionophosphine sulfide - dimer / toluene / 110 °C
3: 75 percent / 20 °C
4: 85 percent / triphenylphosphine / tetrahydrofuran / 16 h / 80 °C
5: 80 percent / Fe, glacial acetic acid / ethanol / 3 h / Heating
With
Lawessons reagent; sulfuric acid; nitric acid; iron; acetic acid; triphenylphosphine;
In
tetrahydrofuran; ethanol; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: p-methoxyphenylthionophosphine sulfide - dimer / toluene / 110 °C
2: 75 percent / 20 °C
3: 85 percent / triphenylphosphine / tetrahydrofuran / 16 h / 80 °C
4: 80 percent / Fe, glacial acetic acid / ethanol / 3 h / Heating
With
Lawessons reagent; iron; acetic acid; triphenylphosphine;
In
tetrahydrofuran; ethanol; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / lead tetraacetate, triethylamine / CH2Cl2 / -20 - 20 °C
2: 75 percent / 20 °C
3: 85 percent / triphenylphosphine / tetrahydrofuran / 16 h / 80 °C
4: 80 percent / Fe, glacial acetic acid / ethanol / 3 h / Heating
With
lead(IV) acetate; iron; acetic acid; triethylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane;