2,3-bis<4-phenyl>-5,8-dimethoxyquinoxaline

Base Information

Chemical Name:2,3-bis<4-phenyl>-5,8-dimethoxyquinoxaline
CAS No.:136270-65-0
Molecular Formula:C₃₂H₃₂Cl₄N₄O₆
Molecular Weight:710.441
Hs Code.:

2,3-bis<4-<N-(2,2-dichloroacetyl)-N-(2-hydroxyethyl)aminomethyl>phenyl>-5,8-dimethoxyquinoxaline

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Chemical Property of 2,3-bis<4-phenyl>-5,8-dimethoxyquinoxaline

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Technology Process of 2,3-bis<4-phenyl>-5,8-dimethoxyquinoxaline

There total 4 articles about 2,3-bis<4-phenyl>-5,8-dimethoxyquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 79-36-7
dichloroacethyl chloride

: 136270-71-8
2-[4-(3-{4-[(2-Hydroxy-ethylamino)-methyl]-phenyl}-5,8-dimethoxy-quinoxalin-2-yl)-benzylamino]-ethanol

: 136270-65-0
2,3-bis<4-phenyl>-5,8-dimethoxyquinoxaline

Guidance literature:: With triethylamine; In 1,4-dioxane; for 1h; Ambient temperature;

Reference yield:

: 6945-76-2
1,4-dimethoxy-2,3-dinitrobenzene

: 136270-65-0
2,3-bis<4-phenyl>-5,8-dimethoxyquinoxaline

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / acetic acid

2: acetic acid / 2.5 h / 90 °C

3: 41 percent / dioxane / 0.5 h / Heating

4: 34 percent / triethylamine / dioxane / 1 h / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; acetic acid;

Reference yield:

: 40328-95-8
2,3-diamino-1,4-dimethoxybenzene

: 136270-65-0
2,3-bis<4-phenyl>-5,8-dimethoxyquinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 2.5 h / 90 °C

2: 41 percent / dioxane / 0.5 h / Heating

3: 34 percent / triethylamine / dioxane / 1 h / Ambient temperature

With triethylamine; In 1,4-dioxane; acetic acid;