1,2-Benzenediamine, 3,6-dimethoxy-

Base Information

• Chemical Name: 1,2-Benzenediamine, 3,6-dimethoxy-
• CAS No.: 40328-95-8
• Molecular Formula: C8H12N2O2
• Molecular Weight: 168.195
• Mol file: 40328-95-8.mol

Synonyms:1,4-dimethoxy-2,3-diaminobenzene;3,6-dimethoxy-1,2-phenylenediamine;2,3-Diamino-1,4-dimethoxybenzene;1,2-diamino-3,6-dimethoxybenzene;3,6-Dimethoxy-benzene-1,2-diamine;2,3-diamino-1,4-dimethoxy-benzene;(3,6-dimethoxy)benzene-1,2-diamine;

Chemical Property of 1,2-Benzenediamine, 3,6-dimethoxy-

Chemical Property:

• PSA: 70.50000
• LogP: 2.03060

Purity/Quality:

99% ^*data from raw suppliers

3,6-Dimethoxybenzene-1,2-diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-Benzenediamine, 3,6-dimethoxy-

There total 7 articles about 1,2-Benzenediamine, 3,6-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,4-dimethoxy-2,3-dinitrobenzene (6945-76-2) → 2,3-diamino-1,4-dimethoxybenzene (40328-95-8)

Guidance literature:

With palladium on carbon; hydrogen; In ethyl acetate; at 20 ℃; under 760.051 Torr;

DOI:10.1021/ol200748c

Reference yield: 97.0%

2-amino-3-nitrohydroquinone dimethylether (26002-57-3) → 2,3-diamino-1,4-dimethoxybenzene (40328-95-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 5h; under 760.051 Torr;

DOI:10.1039/b802649c

Reference yield: 83.0%

1,4-dimethoxybezene (150-78-7) → 2,3-diamino-1,4-dimethoxybenzene (40328-95-8)

Guidance literature:

1,4-dimethoxybezene; With nitric acid; In water; at 0 - 90 ℃;

With 10% palladium on activated carbon; hydrogen; In ethyl acetate;

DOI:10.1055/s-0028-1088049

upstream raw materials:

1,4-dimethoxy-2,3-dinitrobenzene

1,4-dimethoxybezene

2-amino-3-nitrohydroquinone dimethylether

Downstream raw materials:

4,7-Dimethoxy-2-methyl-1H-benzimidazole

5,8-dimethoxy-2,3-diphenylquinoxaline

2,3-bis(4-acetylaminophenyl)-5,8-dimethoxyquinoxaline

2,3-bis(4-bromomethylphenyl)-5,8-dimethoxyquinoxaline