cyclohex-2-enyl phenyl sulfide

Base Information

• Chemical Name: cyclohex-2-enyl phenyl sulfide
• CAS No.: 3467-73-0
• Molecular Formula: C₁₂H₁₄S
• Molecular Weight: 190.309
• Mol file: 3467-73-0.mol

Synonyms:

Chemical Property of cyclohex-2-enyl phenyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclohex-2-enyl phenyl sulfide

There total 13 articles about cyclohex-2-enyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

thiophenol (108-98-5) + Cyclohex-2-enol (822-67-3) → cyclohex-2-enyl phenyl sulfide (134427-69-3,3467-73-0)

Guidance literature:

samarium(III) chloride; In 1,2-dichloro-ethane; for 12h; Heating;

DOI:10.1016/S0040-4020(01)91389-4

Reference yield: 94.0%

thiophenol (108-98-5) + rac-3-bromocyclohexene (1521-51-3,113667-32-6) → cyclohex-2-enyl phenyl sulfide (134427-69-3,3467-73-0)

Guidance literature:

With silver trifluoromethanesulfonate; In acetonitrile; at 0 ℃; for 1h; chemoselective reaction;

DOI:10.1021/acs.joc.1c00480

Reference yield: 92.0%

rac-3-bromocyclohexene (1521-51-3,113667-32-6) + diphenyldisulfane (882-33-7) → cyclohex-2-enyl phenyl sulfide (134427-69-3,3467-73-0)

Guidance literature:

diphenyldisulfane; With zinc; In N,N-dimethyl-formamide; at 110 ℃; for 11h;

rac-3-bromocyclohexene; In N,N-dimethyl-formamide; at 20 ℃;

upstream raw materials:

N-phenyl-benzenesulphenamide

thiophenol

Cyclohex-2-enol

rac-3-bromocyclohexene

Downstream raw materials:

(E/Z)-methyl-3-(phenylthio) acrylate

N-(cyclohex-2-en-1-yl)-4-methyl-N-(phenylthio)benzenesulfonamide

Benzenesulfinic acid

cyclohexa-1,3-diene