[2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

Base Information

• Chemical Name: [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate
• CAS No.: 1420299-69-9
• Molecular Formula: C₃₂H₁₂BF₂₄*C₄₂H₃₇F₃PRuS
• Molecular Weight: 1626.08

Synonyms:

Chemical Property of [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

Chemical Property:

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Technology Process of [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

There total 1 articles about [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]chlorido[tris(4-fluorophenyl)phosphine]ruthenium(II) (1420299-84-8) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate (1420299-69-9)

Guidance literature:

In dichloromethane; at 40 ℃; for 14h;

DOI:10.1021/ja311398j

Reference yield:

[2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate (1420299-69-9) → C42H38F3PRuS (1420299-97-3)

Guidance literature:

With methyldiphenylsilane; sodium methylate; In benzene-d6; at 20 ℃; for 2h;

DOI:10.1021/ja311398j

Reference yield:

[2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate (1420299-69-9) → C42H38F3PRuS (1420299-97-3) + C84H75F6P2Ru2S2(1+)*C32H12BF24(1-) (1420300-01-1)

Guidance literature:

With sodium methylate; diphenyl(methyl)phosphine; In benzene-d6; at 20 ℃; for 2h;

DOI:10.1021/ja311398j

upstream raw materials:

[2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]chlorido[tris(4-fluorophenyl)phosphine]ruthenium(II)

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

Downstream raw materials:

C₄₂H₃₈F₃PRuS

C₈₄H₇₅F₆P₂Ru₂S₂⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-)

C₅₅H₅₁F₃PRuSSi⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-)

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