2-<4--N-methylamino>phenyl>ethyl alcohol

Base Information

Chemical Name:2-<4--N-methylamino>phenyl>ethyl alcohol
CAS No.:126202-87-7
Molecular Formula:C₂₅H₃₀N₂O
Molecular Weight:374.526
Hs Code.:

2-<4-<N-<2-(N-benzhydryl-N-methylamino)ethyl>-N-methylamino>phenyl>ethyl alcohol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<4--N-methylamino>phenyl>ethyl alcohol

Chemical Property:

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Technology Process of 2-<4--N-methylamino>phenyl>ethyl alcohol

There total 4 articles about 2-<4--N-methylamino>phenyl>ethyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 134364-86-6
2-<4-<2-(N-benzhydryl-N-methylamino)ethylamino>phenyl>ethyl alcohol

: 126202-87-7
2-<4--N-methylamino>phenyl>ethyl alcohol

Guidance literature:: With sodium cyanoborohydride; In water; acetonitrile; for 2h; Ambient temperature;
DOI:10.1248/cpb.39.91

Reference yield:

: 101286-71-9
2-(N-benzhydryl-N-methylamino)ethyl alcohol

: 126202-87-7
2-<4--N-methylamino>phenyl>ethyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / DCC, H₃PO₄ / dimethylsulfoxide / 2.5 h / Ambient temperature

2: 51 percent / NaBH₃CN / methanol / 2.5 h / Ambient temperature

3: 66 percent / NaBH₃CN / acetonitrile; H₂O / 2 h / Ambient temperature

With phosphoric acid; sodium cyanoborohydride; dicyclohexyl-carbodiimide; In methanol; water; dimethyl sulfoxide; acetonitrile;
DOI:10.1248/cpb.39.91

Reference yield:

: 126245-53-2
(Benzhydryl-methyl-amino)-acetaldehyde

: 126202-87-7
2-<4--N-methylamino>phenyl>ethyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / NaBH₃CN / methanol / 2.5 h / Ambient temperature

2: 66 percent / NaBH₃CN / acetonitrile; H₂O / 2 h / Ambient temperature

With sodium cyanoborohydride; In methanol; water; acetonitrile;
DOI:10.1248/cpb.39.91