bromo(2-cyanoethyl)diphenylstannane

Base Information

Chemical Name:bromo(2-cyanoethyl)diphenylstannane
CAS No.:157843-36-2
Molecular Formula:C₁₅H₁₄BrNSn
Molecular Weight:406.897
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bromo(2-cyanoethyl)diphenylstannane

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Technology Process of bromo(2-cyanoethyl)diphenylstannane

There total 1 articles about bromo(2-cyanoethyl)diphenylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5827-72-5
3-triphenylstannyl-propionitrile

: 157843-36-2
bromo(2-cyanoethyl)diphenylstannane

Guidance literature:: With Br₂; In petroleum ether; dropwise addn. of soln. of Br2 in light petroleum ether (b.p.: 60-80°C) to soln. of Sn-compd. in the same solvent with stirring; removal of solvent under vac.;
DOI:10.1039/DT9940002135

Reference yield: 67.0%

: 157843-36-2
bromo(2-cyanoethyl)diphenylstannane

: 157843-27-1
2,2-diphenyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

Guidance literature:: With sodium azide; In water; ethyl acetate; Sn-compd. is dissolved in ethyl acetate and placed in a separating funnel, NaN3 is dissolved in water and added to the funnel, shaking for 20 min; sepn. of organic layer, drying over anhydrous Mg2SO4, evapn. of solventunder vac., recrystn. from light petroleum (b.p.: 60-80°C);
DOI:10.1039/DT9940002135

Reference yield:

: 157843-36-2
bromo(2-cyanoethyl)diphenylstannane

: 157843-33-9
2-bromo-2-phenyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / water; ethyl acetate

2: Br₂ / chloroform

With sodium azide; Br₂; In chloroform; water; ethyl acetate;
DOI:10.1039/DT9940002135