5-[2-(chlorodiphenylstannyl)ethyl]tetrazole

Base Information

Chemical Name:5-[2-(chlorodiphenylstannyl)ethyl]tetrazole
CAS No.:157843-30-6
Molecular Formula:C₁₅H₁₅ClN₄Sn
Molecular Weight:405.474
Hs Code.:

Synonyms:5-[2-(chlorodiphenylstannyl)ethyl]tetrazole

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Chemical Property of 5-[2-(chlorodiphenylstannyl)ethyl]tetrazole

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Technology Process of 5-[2-(chlorodiphenylstannyl)ethyl]tetrazole

There total 5 articles about 5-[2-(chlorodiphenylstannyl)ethyl]tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 157843-27-1
2,2-diphenyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

: 157843-30-6
5-[2-(chlorodiphenylstannyl)ethyl]tetrazole

Guidance literature:: In methanol; Sn-compd. is suspended in boiling MeOH, dropwise addn. of aq. HCl (5 min) with stirring, further stirring for 10 min; slow cooling to 0°C for crystn., elem. anal.;
DOI:10.1039/DT9940002135

Reference yield: 85.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 157843-26-0
2-(tributylstannyl)-5-[2-(triphenylstannyl)ethyl]tetrazole

: 157843-30-6
5-[2-(chlorodiphenylstannyl)ethyl]tetrazole

: 1461-22-9
tributyltin chloride

Guidance literature:: In methanol; Sn-compd. and aq. HCl are dissolved in MeOH and stirred at room temp. for 1 h; evapn. of solvent under vac., trituration with Et2O, filtn., recrystn. from MeOH, the ether soluble filtrate contains SnBu3Cl;
DOI:10.1039/DT9940002135

Reference yield:

: 5827-72-5
3-triphenylstannyl-propionitrile

: 157843-30-6
5-[2-(chlorodiphenylstannyl)ethyl]tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: neat (no solvent)

2: neat (no solvent)

3: methanol

In methanol;
DOI:10.1039/DT9940002135