1,3-Bis--adamantan

Base Information

• Chemical Name: 1,3-Bis--adamantan
• CAS No.: 4933-53-3
• Molecular Formula: C₂₄H₂₈O₂
• Molecular Weight: 348.485

Synonyms:

Chemical Property of 1,3-Bis--adamantan

Chemical Property:

Purity/Quality:

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Technology Process of 1,3-Bis--adamantan

There total 3 articles about 1,3-Bis--adamantan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

dinitrate of 1,3-adamantanediol (53488-28-1) + methoxybenzene (100-66-3) → 1,3-Bis--adamantan (4933-53-3)

Guidance literature:

With sulfuric acid; for 1h; Ambient temperature;

Reference yield:

methoxybenzene (100-66-3) + 3-methylenebicyclo<3.3.1>nonan-7-one → 1,3-Bis--adamantan (4933-53-3)

Guidance literature:

With toluene-4-sulfonic acid; Heating;

Reference yield:

→ 1,3-Bis--adamantan (4933-53-3)

Guidance literature:

Adamantan-1,3-diol, 1) Anisol / H2SO4 (18-20grad; 1,5h); 2) Extrahieren Toluol; 3) NaHCO3; 4) H2O; 5) Kristalle aus Heptan;

upstream raw materials:

dinitrate of 1,3-adamantanediol

methoxybenzene

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