Technology Process of 4-benzoyl-2-methyl-benzonitrile
There total 4 articles about 4-benzoyl-2-methyl-benzonitrile which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: PCl5; benzene / Erwaermen des erhaltenen 4-Nitro-3-methyl-benzoylchlorids mit Benzol und AlCl3 auf 40-50grad
2: sodium sulfide; aqueous ethanol
3: aqueous hydrochloric acid; sodium nitrite / Diazotization.Erwaermen der Diazoniumsalz-Loesung mit einer aus Kaliumcyanid, Kupfer(II)-sulfat und Wasser hergestellten Loesung
With
hydrogenchloride; sodium sulfide; ethanol; phosphorus pentachloride; sodium nitrite; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium sulfide; aqueous ethanol
2: aqueous hydrochloric acid; sodium nitrite / Diazotization.Erwaermen der Diazoniumsalz-Loesung mit einer aus Kaliumcyanid, Kupfer(II)-sulfat und Wasser hergestellten Loesung
With
hydrogenchloride; sodium sulfide; ethanol; sodium nitrite;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: zinc chloride / 220 °C
2: aqueous hydrochloric acid; sodium nitrite / Diazotization.Erwaermen der Diazoniumsalz-Loesung mit einer aus Kaliumcyanid, Kupfer(II)-sulfat und Wasser hergestellten Loesung
With
hydrogenchloride; zinc(II) chloride; sodium nitrite;