Technology Process of Acetic acid 4-[2-(4-chloro-benzoylamino)-phenylsulfanyl]-benzyl ester
There total 8 articles about Acetic acid 4-[2-(4-chloro-benzoylamino)-phenylsulfanyl]-benzyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
benzene;
for 2h;
Heating;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) NBS, benzoyl-peroxide; 2.) silver nitrate / 1.) CCl4, reflux, 15 h; 2.) acetone, water, room temp., 1 h
2: 70 percent / NaBH4 / ethanol / 1 h / Ambient temperature
3: 73 percent / Et3N / benzene / 0.5 h / Ambient temperature
4: 84 percent / hydrogen / Ni / ethanol / 4 h / 60 °C / 77572.2 Torr
5: 81 percent / triethylamine / benzene / 2 h / Heating
With
sodium tetrahydroborate; N-Bromosuccinimide; Perbenzoic acid; hydrogen; silver nitrate; triethylamine;
nickel;
In
ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 89 percent / sodium ethylate / ethanol / 3 h / Ambient temperature
2: 1.) NBS, benzoyl-peroxide; 2.) silver nitrate / 1.) CCl4, reflux, 15 h; 2.) acetone, water, room temp., 1 h
3: 70 percent / NaBH4 / ethanol / 1 h / Ambient temperature
4: 73 percent / Et3N / benzene / 0.5 h / Ambient temperature
5: 84 percent / hydrogen / Ni / ethanol / 4 h / 60 °C / 77572.2 Torr
6: 81 percent / triethylamine / benzene / 2 h / Heating
With
sodium tetrahydroborate; N-Bromosuccinimide; Perbenzoic acid; hydrogen; sodium ethanolate; silver nitrate; triethylamine;
nickel;
In
ethanol; benzene;