2-n-butoxy-6--propionamide>-benzothiazole

Base Information

Chemical Name:2-n-butoxy-6--propionamide>-benzothiazole
CAS No.:77563-15-6
Molecular Formula:C₂₉H₄₀N₄O₂S
Molecular Weight:508.728
Hs Code.:

2-n-butoxy-6-<N-<1-methyl-2-(4-phenethylpiperazino)ethyl>-propionamide>-benzothiazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-n-butoxy-6--propionamide>-benzothiazole

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Technology Process of 2-n-butoxy-6--propionamide>-benzothiazole

There total 4 articles about 2-n-butoxy-6--propionamide>-benzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.8%

: 123-62-6
propionic acid anhydride

: 77563-09-8
6-<1-methyl-2-(4-phenethylpiperazino)ethyl>-amino-2-n-butoxy-benzothiazole

: 77563-15-6
2-n-butoxy-6--propionamide>-benzothiazole

Guidance literature:: at 100 ℃; for 3h;
DOI:10.1248/cpb.28.3315

Reference yield:

: 5321-49-3
4-(phenethyl)piperazine

: 77563-15-6
2-n-butoxy-6--propionamide>-benzothiazole

Guidance literature:: Multi-step reaction with 4 steps

1: 16 g / benzene / 2 h / 5 °C

2: 55.9 percent / K₂CO₃ / ethanol / 5.5 h / Heating

3: 95.4 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 5 h / Heating

4: 57.8 percent / 3 h / 100 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; diethyl ether; ethanol; benzene;
DOI:10.1248/cpb.28.3315

Reference yield:

: 77563-32-7
1-<2-(2-n-butoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

: 77563-15-6
2-n-butoxy-6--propionamide>-benzothiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 95.4 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 5 h / Heating

2: 57.8 percent / 3 h / 100 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1248/cpb.28.3315