C₂₀H₁₅N₃O₃

Base Information

Chemical Name:C₂₀H₁₅N₃O₃
CAS No.:1426934-85-1
Molecular Formula:C₂₀H₁₅N₃O₃
Molecular Weight:345.357
Hs Code.:

C<sub>20</sub>H<sub>15</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₀H₁₅N₃O₃

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Technology Process of C₂₀H₁₅N₃O₃

There total 7 articles about C₂₀H₁₅N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1426934-83-9
ethyl 1-(4-methoxybenzyl)-6-phenyl-1H-pyrazolo[3,4-b]pyridine-4-carboxylate

: 1426934-85-1
C₂₀H₁₅N₃O₃

Guidance literature:: With boron dimethyl-trifluoro sulphide; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/jm301709s

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1426934-85-1
C₂₀H₁₅N₃O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrazine hydrate / ethanol / 24 h / 0 - 20 °C

1.2: 2 h / 0 - 20 °C

2.1: sodium butanolate / butan-1-ol / 3 h / 120 °C

3.1: benzene / 20 h / 65 °C

4.1: acetic acid / 3 h / Reflux

5.1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 4 h / -78 - 0 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,4-dioxane / 5 h / 100 °C

7.1: boron dimethyl-trifluoro sulphide / dichloromethane / 18 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; boron dimethyl-trifluoro sulphide; caesium carbonate; hydrazine hydrate; acetic acid; sodium butanolate; In 1,4-dioxane; ethanol; dichloromethane; butan-1-ol; benzene; 6.1: |Suzuki Coupling;
DOI:10.1021/jm301709s

Reference yield:

: 64841-16-3
3-{N'-[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-propionitrile

: 1426934-85-1
C₂₀H₁₅N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1: sodium butanolate / butan-1-ol / 3 h / 120 °C

2: benzene / 20 h / 65 °C

3: acetic acid / 3 h / Reflux

4: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 4 h / -78 - 0 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,4-dioxane / 5 h / 100 °C

6: boron dimethyl-trifluoro sulphide / dichloromethane / 18 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; boron dimethyl-trifluoro sulphide; caesium carbonate; acetic acid; sodium butanolate; In 1,4-dioxane; dichloromethane; butan-1-ol; benzene; 5: |Suzuki Coupling;
DOI:10.1021/jm301709s