C₁₉H₂₉N₂O₃P

Base Information

Chemical Name:C₁₉H₂₉N₂O₃P
CAS No.:1577258-75-3
Molecular Formula:C₁₉H₂₉N₂O₃P
Molecular Weight:364.425
Hs Code.:

C<sub>19</sub>H<sub>29</sub>N<sub>2</sub>O<sub>3</sub>P

Synonyms:

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Chemical Property of C₁₉H₂₉N₂O₃P

Chemical Property:

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Technology Process of C₁₉H₂₉N₂O₃P

There total 6 articles about C₁₉H₂₉N₂O₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-97-8
3,3-dimethyl-butan-2-one

: 1577258-75-3
C₁₉H₂₉N₂O₃P

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / diethyl ether / 0.5 h / 10 °C / Cooling with ice; Inert atmosphere

2: toluene / 48 h / 80 °C / Inert atmosphere

3: hydrogen; palladium 10% on activated carbon / methanol / 18 h / 760.05 Torr / Inert atmosphere

4: potassium phosphate / water; dichloromethane / 2 h / Cooling with ice; Inert atmosphere

5: triethylamine; phosphorus trichloride / pentane / 6 h / -78 - 20 °C / Inert atmosphere

6: benzene-d6 / 12 h / 20 °C / Inert atmosphere; Sealed tube

With potassium phosphate; palladium 10% on activated carbon; hydrogen; bromine; triethylamine; phosphorus trichloride; In methanol; diethyl ether; dichloromethane; benzene-d6; water; toluene; pentane;
DOI:10.1021/ja412469e

Reference yield:

: 88686-46-8
5-aza-2,2,8,8-tetramethylnonane-3,7-dione

: 1577258-75-3
C₁₉H₂₉N₂O₃P

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; phosphorus trichloride / pentane / 6 h / -78 - 20 °C / Inert atmosphere

2: benzene-d6 / 12 h / 20 °C / Inert atmosphere; Sealed tube

With triethylamine; phosphorus trichloride; In benzene-d6; pentane;
DOI:10.1021/ja412469e

Reference yield:

: 105858-00-2
5-aza-5-benzyl-2,2,8,8-tetramethylnonane-3,7-dione hydrobromide

: 1577258-75-3
C₁₉H₂₉N₂O₃P

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; palladium 10% on activated carbon / methanol / 18 h / 760.05 Torr / Inert atmosphere

2: potassium phosphate / water; dichloromethane / 2 h / Cooling with ice; Inert atmosphere

3: triethylamine; phosphorus trichloride / pentane / 6 h / -78 - 20 °C / Inert atmosphere

4: benzene-d6 / 12 h / 20 °C / Inert atmosphere; Sealed tube

With potassium phosphate; palladium 10% on activated carbon; hydrogen; triethylamine; phosphorus trichloride; In methanol; dichloromethane; benzene-d6; water; pentane;
DOI:10.1021/ja412469e