C₅₄H₅₀P₃Re, light brown

Base Information

Chemical Name:C₅₄H₅₀P₃Re, light brown
CAS No.:12104-75-5
Molecular Formula:C₅₄H₅₀P₃Re
Molecular Weight:978.119
Hs Code.:

C<sub>54</sub>H<sub>50</sub>P<sub>3</sub>Re, light brown

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Chemical Property of C₅₄H₅₀P₃Re, light brown

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Technology Process of C₅₄H₅₀P₃Re, light brown

There total 7 articles about C₅₄H₅₀P₃Re, light brown which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 12103-40-1
bis(triphenylphosphine)-rhenium heptahydride

: 12104-75-5,122169-15-7
pentahydridotris(triphenylphosphane)Re(V)

Guidance literature:: With triphenylphosphine; In benzene; heated to 50°C for 2 h under inert atmosphere; solvent was removed under vac. and replaced with ether, crystals pptd. as the ether slowly evapd., these were washed with hexane and dried under vac.;

Reference yield: 61.0%

: 16940-66-2
sodium tetrahydroborate

: [ReOCl₃(PPh₃)₂]

: 12104-75-5,122169-15-7
pentahydridotris(triphenylphosphane)Re(V)

Guidance literature:: With P(C₆H₅)3; In ethanol; N2-atmosphere; excess of NaBH4, refluxing for 3 h; filtration, extn. into PhMe, evapn. (vac.), washing (MeOH, Et2O);
DOI:10.1039/DT9950003153

Reference yield: 61.0%

: 16940-66-2
sodium tetrahydroborate

: [ReOCl₃(PPh₃)₂]

: 603-35-0
triphenylphosphine

: 12104-75-5,122169-15-7
pentahydridotris(triphenylphosphane)Re(V)

Guidance literature:: In ethanol; (N2); reflux (3 h), filtration, extn. (toluene), solvent evapn. (vacuum); washing (methanol, diethyl ether);
DOI:10.1016/0277-5387(95)00304-4