2-(3-benzyloxyethyl)-3-ethoxy-1-methylcyclohexene

Base Information

• Chemical Name: 2-(3-benzyloxyethyl)-3-ethoxy-1-methylcyclohexene
• CAS No.: 110526-43-7
• Molecular Formula: C₁₈H₂₆O₂
• Molecular Weight: 274.403
• Mol file: 110526-43-7.mol

Synonyms:

Chemical Property of 2-(3-benzyloxyethyl)-3-ethoxy-1-methylcyclohexene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(3-benzyloxyethyl)-3-ethoxy-1-methylcyclohexene

There total 7 articles about 2-(3-benzyloxyethyl)-3-ethoxy-1-methylcyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-carbethoxy-3-methyl-2-cyclohexen-1-one (487-51-4) → 2-(3-benzyloxyethyl)-3-ethoxy-1-methylcyclohexene (110526-43-7)

Guidance literature:

Multi-step reaction with 5 steps

1: NaH / dimethylformamide

2: KOH / ethanol

3: 93.9 percent / LiAlH₄ / diethyl ether

4: 94.6 percent / pyridine

5: 45 percent Chromat_. / 80 percent aq. ethanol / 50 °C

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; ethanol; sodium hydride; In diethyl ether; ethanol; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)89944-0

Reference yield:

bromoethyl-2-benzyl ether (1462-37-9) → 2-(3-benzyloxyethyl)-3-ethoxy-1-methylcyclohexene (110526-43-7)

Guidance literature:

Multi-step reaction with 5 steps

1: NaH / dimethylformamide

2: KOH / ethanol

3: 93.9 percent / LiAlH₄ / diethyl ether

4: 94.6 percent / pyridine

5: 45 percent Chromat_. / 80 percent aq. ethanol / 50 °C

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; ethanol; sodium hydride; In diethyl ether; ethanol; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)89944-0

Reference yield:

2-(2-benzyloxyethyl)-3-methyl-2-cyclohexenone (110526-19-7) → 2-(3-benzyloxyethyl)-3-ethoxy-1-methylcyclohexene (110526-43-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 93.9 percent / LiAlH₄ / diethyl ether

2: 94.6 percent / pyridine

3: 45 percent Chromat_. / 80 percent aq. ethanol / 50 °C

With pyridine; lithium aluminium tetrahydride; ethanol; In diethyl ether;

DOI:10.1016/S0040-4020(01)89944-0

upstream raw materials:

ethanol

2-(2-benzyloxyethyl)-3-methyl-2-cyclohexenyl p-nitrobenzoate

4-carbethoxy-3-methyl-2-cyclohexen-1-one

bromoethyl-2-benzyl ether