2-(methylthio)-3-buten-2-yl p-tolyl sulfate

Base Information

Chemical Name:2-(methylthio)-3-buten-2-yl p-tolyl sulfate
CAS No.:99946-89-1
Molecular Formula:C₁₂H₁₆O₂S₂
Molecular Weight:256.39
Hs Code.:

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Chemical Property of 2-(methylthio)-3-buten-2-yl p-tolyl sulfate

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Technology Process of 2-(methylthio)-3-buten-2-yl p-tolyl sulfate

There total 3 articles about 2-(methylthio)-3-buten-2-yl p-tolyl sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94816-47-4
1-(methylthio)-1-propyl p-tolyl sulfone

: 99946-89-1
2-(methylthio)-3-buten-2-yl p-tolyl sulfate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / SO₂Cl₂ / CHCl₃ / 1.) 0 deg C, 1.5 h, 2.) RT, 2 h

2: 87 percent / toluene / 22.5 h / Heating

3: NaH / dimethylformamide / 1.) 0 deg C, 6 h, 2.) RT, 18 h

With sulfuryl dichloride; sodium hydride; In chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo00355a021

Reference yield:

: 99946-81-3
1-chloro-1-(methylthio)-1-propyl p-tolyl sulfone

: 99946-89-1
2-(methylthio)-3-buten-2-yl p-tolyl sulfate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / toluene / 22.5 h / Heating

2: NaH / dimethylformamide / 1.) 0 deg C, 6 h, 2.) RT, 18 h

With sodium hydride; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo00355a021