(R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol

Base Information

Chemical Name:(R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol
CAS No.:205587-49-1
Molecular Formula:C₃₂H₅₅NO₅Si₂
Molecular Weight:589.963
Hs Code.:

Synonyms:

Suppliers and Price of (R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol

There total 12 articles about (R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40167-10-0
2-[4-(benzyloxy)phenyl]acetaldehyde

: 205587-49-1
(R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / tetrahydrofuran

2: 94 percent / H₂ / 10percent Pd-C / ethanol

3: 96 percent / NaH / dimethylformamide

4: 100 percent / LiOH / methanol; H₂O

5: 82 percent / DEPC, Et₃N / dimethylformamide / from 0 deg to RT

6: LiAlH₄ / diethyl ether / Heating

With lithium hydroxide; lithium aluminium tetrahydride; hydrogen; sodium hydride; triethylamine; diethyl dicarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide;
DOI:10.3987/com-97-s55

Reference yield:

: 501-94-0
p-hydroxyphenethyl alcohol

: 205587-49-1
(R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol

Guidance literature:: Multi-step reaction with 8 steps

1: 96 percent / K₂CO₃ / methanol

2: 88 percent / Dess-Martin / CH₂Cl₂

3: 84 percent / tetrahydrofuran

4: 94 percent / H₂ / 10percent Pd-C / ethanol

5: 96 percent / NaH / dimethylformamide

6: 100 percent / LiOH / methanol; H₂O

7: 82 percent / DEPC, Et₃N / dimethylformamide / from 0 deg to RT

8: LiAlH₄ / diethyl ether / Heating

With lithium hydroxide; lithium aluminium tetrahydride; hydrogen; sodium hydride; potassium carbonate; Dess-Martin periodane; triethylamine; diethyl dicarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.3987/com-97-s55

Reference yield:

: 61439-59-6
2-(4-benzyloxyphenyl)ethanol

: 205587-49-1
(R)-1-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-[4-(4-methoxymethoxy-phenyl)-butylamino]-ethanol

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / Dess-Martin / CH₂Cl₂

2: 84 percent / tetrahydrofuran

3: 94 percent / H₂ / 10percent Pd-C / ethanol

4: 96 percent / NaH / dimethylformamide

5: 100 percent / LiOH / methanol; H₂O

6: 82 percent / DEPC, Et₃N / dimethylformamide / from 0 deg to RT

7: LiAlH₄ / diethyl ether / Heating

With lithium hydroxide; lithium aluminium tetrahydride; hydrogen; sodium hydride; Dess-Martin periodane; triethylamine; diethyl dicarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.3987/com-97-s55