Benzenepropanoic acid, a-methyl-b-(trimethylstannyl)-, methyl ester

Base Information

Chemical Name:Benzenepropanoic acid, a-methyl-b-(trimethylstannyl)-, methyl ester
CAS No.:106119-84-0
Molecular Formula:C₁₄H₂₂O₂Sn
Molecular Weight:341.037
Hs Code.:

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Chemical Property of Benzenepropanoic acid, a-methyl-b-(trimethylstannyl)-, methyl ester

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Technology Process of Benzenepropanoic acid, a-methyl-b-(trimethylstannyl)-, methyl ester

There total 1 articles about Benzenepropanoic acid, a-methyl-b-(trimethylstannyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21370-57-0,22946-43-6,25692-59-5
methyl 2-methyl-3-phenylacrylate

: 1631-73-8
trimethylstannane

: 106119-84-0
(CH₃)3SnCHCH₃CHC₆H₅COOCH₃

Guidance literature:: In neat (no solvent); Irradiation (UV/VIS); under N2, ratio Me3SnH : olefin = 1.5:1, olefin added to Me3SnH, stirred for 60 min at 25°C; ratio of enantiomers 20:80, separated by column chromy. on silica gel, elem. anal.;
DOI:10.1021/om00125a013

Reference yield: 100.0%

: 106119-84-0
(CH₃)3SnCHCH₃CHC₆H₅COOCH₃

: 2857-97-8
trimethylsilyl bromide

: (CH₃)2SnBrCHCH₃CHC₆H₅COOCH₃

Guidance literature:: In tetrachloromethane; byproducts: (CH3)4Si; N2 atmosphere; 65 ° C; 26 h; organotin ester/(CH3)3SiBr ratio = 1/4; solvent distillation; elem. anal.;
DOI:10.1016/S0022-328X(00)99028-4

Reference yield:

: 106119-84-0
(CH₃)3SnCHCH₃CHC₆H₅COOCH₃

: 1066-45-1
trimethyltin(IV)chloride

: (CH₃)2ClSnHC(C₆H₅)CH(CH₃)COOCH₃

Guidance literature:: In neat (no solvent); byproducts: (CH3)4Sn; under N2, Me3SnCH-compd. added to Me3SnCl with a ratio of 1:1.2 with stirring, left at room temp. for 22 or 20 h;
DOI:10.1021/om00125a013