trans-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

Base Information

Chemical Name:trans-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂
CAS No.:141666-73-1
Molecular Formula:C₃₂H₃₆Cl₂O₃P₂Pt
Molecular Weight:796.57
Hs Code.:

trans-Ph<sub>2</sub>P(CH<sub>2</sub>CH<sub>2</sub>O)3CH<sub>2</sub>CH<sub>3</sub>PPh<sub>2</sub>-P,P')PtCl<sub>2</sub>

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Chemical Property of trans-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

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Technology Process of trans-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

There total 4 articles about trans-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.8%

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

: 98583-60-9
2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

: 141666-73-1
cis-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

: 141666-73-1
trans-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

Guidance literature:: In dichloromethane; ligand in CH2Cl2 slowly added to soln. of Pt complex in CH2Cl2, stirred at ambient temp. for 20 h; concd., poured into hexane, pptd., washed (hexanes), dried (vac.) at 298K for 48 h, chromy.(silica gel - ethyl acetate 5:1), recrystd.(hexane/C H2Cl2), elem. anal.;
DOI:10.1002/ejic.200800436

Reference yield: 39.8%

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

: 98583-60-9
2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

: 141666-73-1
cis-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

: 141666-73-1
trans-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

Guidance literature:: In dichloromethane; ligand in CH2Cl2 slowly added to soln. of Pt complex in CH2Cl2, stirred at ambient temp. for 20 h; concd., poured into hexane, pptd., washed (hexanes), dried (vac.) at 298K for 48 h, chromy.(silica gel - ethyl acetate 5:1), recrystd.(hexane/C H2Cl2), elem. anal.;
DOI:10.1002/ejic.200800436

Reference yield:

: 141666-73-1
trans-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

: 141666-73-1
cis-Ph₂P(CH₂CH₂O)3CH₂CH₃PPh₂-P,P')PtCl₂

Guidance literature:: With DCl; In water-d2; a drop of DCl in D2O added to soln. of cis-Pt complex dissolved in 1,2-d2-tetrachloroethane, preheated at 75°C for 30 min, equilibrated at isomerized at 331-348 K; Kinetics;
DOI:10.1002/ejic.200800436