2,7,12-Tris-(3,5-dibrom-2-methoxyphenyl)-4,4a,9,9a,14,14a-hexahydro-3H,8H,13H-tripyradizino<1,6-a:1',6'-c:1',6'-e>-s-triazin

Base Information

Chemical Name:2,7,12-Tris-(3,5-dibrom-2-methoxyphenyl)-4,4a,9,9a,14,14a-hexahydro-3H,8H,13H-tripyradizino<1,6-a:1',6'-c:1',6'-e>-s-triazin
CAS No.:121789-72-8
Molecular Formula:C₃₃H₃₀Br₆N₆O₃
Molecular Weight:1038.06
Hs Code.:

Synonyms:

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Chemical Property of 2,7,12-Tris-(3,5-dibrom-2-methoxyphenyl)-4,4a,9,9a,14,14a-hexahydro-3H,8H,13H-tripyradizino<1,6-a:1',6'-c:1',6'-e>-s-triazin

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Technology Process of 2,7,12-Tris-(3,5-dibrom-2-methoxyphenyl)-4,4a,9,9a,14,14a-hexahydro-3H,8H,13H-tripyradizino<1,6-a:1',6'-c:1',6'-e>-s-triazin

There total 9 articles about 2,7,12-Tris-(3,5-dibrom-2-methoxyphenyl)-4,4a,9,9a,14,14a-hexahydro-3H,8H,13H-tripyradizino<1,6-a:1',6'-c:1',6'-e>-s-triazin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 121789-40-0
1-(3,5-Dibrom-2-methoxyphenyl)-1,4-butandion

: 121789-72-8
2,7,12-Tris-(3,5-dibrom-2-methoxyphenyl)-4,4a,9,9a,14,14a-hexahydro-3H,8H,13H-tripyradizino<1,6-a:1',6'-c:1',6'-e>-s-triazin

Guidance literature:: With hydrazine hydrate; In acetic acid; for 0.166667h;

Reference yield:

: 13130-23-9
3,5-dibromo-2-methoxybenzoic acid

: 121789-72-8
2,7,12-Tris-(3,5-dibrom-2-methoxyphenyl)-4,4a,9,9a,14,14a-hexahydro-3H,8H,13H-tripyradizino<1,6-a:1',6'-c:1',6'-e>-s-triazin

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 1 h / Heating

2: 1.) Mg

3: 1.) glacial acetic acid, conc. HCl; 2.) glacial acetic acid, conc. HCl / 1.) water, 3 d, RT; 2.) water, 3 d, RT

4: 67 percent / 80percent hydrazine / acetic acid / 0.17 h

With hydrogenchloride; thionyl chloride; hydrazine hydrate; magnesium; acetic acid; In acetic acid;

Reference yield:

: 15790-59-7
3,5-dibromo-2-methoxy-benzoic acid methyl ester

: 121789-72-8
2,7,12-Tris-(3,5-dibrom-2-methoxyphenyl)-4,4a,9,9a,14,14a-hexahydro-3H,8H,13H-tripyradizino<1,6-a:1',6'-c:1',6'-e>-s-triazin

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / KOH / methanol; H₂O / 4 h / Heating

2: thionyl chloride / 1 h / Heating

3: 1.) Mg

4: 1.) glacial acetic acid, conc. HCl; 2.) glacial acetic acid, conc. HCl / 1.) water, 3 d, RT; 2.) water, 3 d, RT

5: 67 percent / 80percent hydrazine / acetic acid / 0.17 h

With hydrogenchloride; potassium hydroxide; thionyl chloride; hydrazine hydrate; magnesium; acetic acid; In methanol; water; acetic acid;