C₂₄H₂₈O₂S

Base Information

Chemical Name:C₂₄H₂₈O₂S
CAS No.:98115-53-8
Molecular Formula:C₂₄H₂₈O₂S
Molecular Weight:380.551
Hs Code.:

C<sub>24</sub>H<sub>28</sub>O<sub>2</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₈O₂S

Chemical Property:

Purity/Quality:

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Technology Process of C₂₄H₂₈O₂S

There total 16 articles about C₂₄H₂₈O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1199-31-1
1-cyano-5-methoxybenzocyclobutane

: 98115-53-8,98243-17-5
C₂₄H₂₈O₂S

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / -78 °C

2: 73 percent / toluene-p-sulphonic acid / benzene / 2 h / Heating

3: 80 percent / liq. NH₃, sodium / ethanol; tetrahydrofuran / 3 h / -78 °C

4: 78 percent / 10percent HCl / methanol / 5 h / Ambient temperature

5: 52 percent / Et₃N / 12 h / Ambient temperature

6: 62 percent / tetrahydrofuran / 1 h / 0 °C

7: 2.) MCPBA / 1.) 1,2-dichlorobenzene, reflux, 5 h.; 2.) methylene dichloride, room temp., 30 min.

With hydrogenchloride; ammonia; sodium; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; benzene;

Reference yield:

: 1199-31-1
1-cyano-5-methoxybenzocyclobutane

: 98115-53-8,98243-17-5
C₂₄H₂₈O₂S

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / -78 °C

2: 73 percent / toluene-p-sulphonic acid / benzene / 2 h / Heating

3: 80 percent / liq. NH₃, sodium / ethanol; tetrahydrofuran / 3 h / -78 °C

4: 78 percent / 10percent HCl / methanol / 5 h / Ambient temperature

5: 52 percent / Et₃N / 12 h / Ambient temperature

6: 62 percent / tetrahydrofuran / 1 h / 0 °C

7: 2.) MCPBA / 1.) 1,2-dichlorobenzene, reflux, 5 h.; 2.) methylene dichloride, room temp., 30 min.

With hydrogenchloride; ammonia; sodium; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; benzene;

Reference yield:

: 98115-47-0
1-cyano-5-methoxy-1-(2-methyl-4-oxocyclohex-1-enylmethyl)-1,2-dihydrocyclobutabenzene

: 98115-53-8,98243-17-5
C₂₄H₂₈O₂S

Guidance literature:: Multi-step reaction with 6 steps

1: 73 percent / toluene-p-sulphonic acid / benzene / 2 h / Heating

2: 80 percent / liq. NH₃, sodium / ethanol; tetrahydrofuran / 3 h / -78 °C

3: 78 percent / 10percent HCl / methanol / 5 h / Ambient temperature

4: 52 percent / Et₃N / 12 h / Ambient temperature

5: 62 percent / tetrahydrofuran / 1 h / 0 °C

6: 2.) MCPBA / 1.) 1,2-dichlorobenzene, reflux, 5 h.; 2.) methylene dichloride, room temp., 30 min.

With hydrogenchloride; ammonia; sodium; triethylamine; 3-chloro-benzenecarboperoxoic acid; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; benzene;