5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol

Base Information

Chemical Name:5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol
CAS No.:863986-18-9
Molecular Formula:C₂₀H₂₈O₇
Molecular Weight:380.438
Hs Code.:

Synonyms:

Suppliers and Price of 5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol

Chemical Property:

Purity/Quality:

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Technology Process of 5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol

There total 3 articles about 5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156556-46-6
2-O-benzoyl-myo-inositol

: 863986-18-9
5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 1.5 h / 50 °C / Inert atmosphere

2: silver(l) oxide; tetra-(n-butyl)ammonium iodide / dichloromethane / 24 h / 20 °C / Molecular sieve

3: sodium methylate; methanol / 4 h / 20 °C / Inert atmosphere

With methanol; sodium methylate; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; silver(l) oxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c6ob00094k

Reference yield:

: 208714-30-1
2-O-benzoyl-1,6:3,4-di-O-isopropylidene-myo-inositol

: 863986-18-9
5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: silver(l) oxide; tetra-(n-butyl)ammonium iodide / dichloromethane / 24 h / 20 °C / Molecular sieve

2: sodium methylate; methanol / 4 h / 20 °C / Inert atmosphere

With methanol; sodium methylate; tetra-(n-butyl)ammonium iodide; silver(l) oxide; In dichloromethane;
DOI:10.1039/c6ob00094k

Reference yield:

: 87-89-8
D-myo-inositol

: 863986-18-9
5-O-(4-methoxybenzyl)-1,6:3,4-di-O-isopropylidene-myo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1.1: camphor-10-sulfonic acid; dimethyl sulfoxide / 5 h / 80 °C / 187.52 Torr / Inert atmosphere

1.2: 0.17 h / 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 1.5 h / 50 °C / Inert atmosphere

3.1: silver(l) oxide; tetra-(n-butyl)ammonium iodide / dichloromethane / 24 h / 20 °C / Molecular sieve

4.1: sodium methylate; methanol / 4 h / 20 °C / Inert atmosphere

With methanol; camphor-10-sulfonic acid; sodium methylate; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; dimethyl sulfoxide; silver(l) oxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c6ob00094k