(+)-(R)_p Methyl methylphenylthiophosphinate

Base Information

Chemical Name:(+)-(R)_p Methyl methylphenylthiophosphinate
CAS No.:78037-58-8
Molecular Formula:C₈H₁₁OPS
Molecular Weight:186.214
Hs Code.:

(+)-(R)<sub>p</sub> Methyl methylphenylthiophosphinate

Synonyms:

Suppliers and Price of (+)-(R)_p Methyl methylphenylthiophosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(R)_p Methyl methylphenylthiophosphinate

Chemical Property:

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Technology Process of (+)-(R)_p Methyl methylphenylthiophosphinate

There total 5 articles about (+)-(R)_p Methyl methylphenylthiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 78037-58-8
(+)-(R)_p Methyl methylphenylthiophosphinate

Guidance literature:: With sulfuric acid; In methanol; for 2h; Yield given; Heating; ee 99percent;
DOI:10.1016/S0040-4039(01)90157-1

Reference yield:

: 38605-11-7
(+)R-S-methyl methylphenylphosphinothiolate

: 78037-58-8
(+)-(R)_p Methyl methylphenylthiophosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent Spectr_. / CH₂Cl₂ / 0.25 h / Heating

2: 0.04 g / NaSH / diethyl ether / -70 deg C, 1 h then rt.

With sodium hydrogensulfide; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)81908-6