Technology Process of 2-N-Benzoyl-1',2'-di-O-benzoyl-4-thiobiopterin
There total 5 articles about 2-N-Benzoyl-1',2'-di-O-benzoyl-4-thiobiopterin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid; ethanol / Ambient temperature
2: 2) K4, KI, 30percent H2O2 / 1) aq. CH3OH, 2 h, RT; 1 h, reflux, 2) 15 h
3: 74 percent / pyridine / 0.25 h / Heating
4: 1) P4S10, 2) H2O / 1) pyridine, reflux, 2) pyridine, reflux, 25 h
With
tetraphosphorus decasulfide; water; dihydrogen peroxide; potassium iodide; potassium ferrocyanide;
In
pyridine; ethanol; acetic acid;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 74 percent / pyridine / 0.25 h / Heating
2: 1) P4S10, 2) H2O / 1) pyridine, reflux, 2) pyridine, reflux, 25 h
With
tetraphosphorus decasulfide; water;
In
pyridine;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2) K4, KI, 30percent H2O2 / 1) aq. CH3OH, 2 h, RT; 1 h, reflux, 2) 15 h
2: 74 percent / pyridine / 0.25 h / Heating
3: 1) P4S10, 2) H2O / 1) pyridine, reflux, 2) pyridine, reflux, 25 h
With
tetraphosphorus decasulfide; water; dihydrogen peroxide; potassium iodide; potassium ferrocyanide;
In
pyridine;