C₂₀H₂₈O₄

Base Information

Chemical Name:C₂₀H₂₈O₄
CAS No.:1353667-15-8
Molecular Formula:C₂₀H₂₈O₄
Molecular Weight:332.44
Hs Code.:

C<sub>20</sub>H<sub>28</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₈O₄

Chemical Property:

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Technology Process of C₂₀H₂₈O₄

There total 4 articles about C₂₀H₂₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353667-13-6
C₂₂H₃₂O₆

: 1353667-15-8
C₂₀H₂₈O₄

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide pentahydrate; water / tetrahydrofuran / 4 h / 0 - 20 °C

2: tetrachloromethane; sodium hydrogencarbonate; triphenylphosphine / 48 h / Reflux

3: ammonia; lithium; ferric nitrate / 2 h / -40 °C

With tetrachloromethane; lithium hydroxide pentahydrate; ammonia; water; lithium; sodium hydrogencarbonate; ferric nitrate; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2011.10.117

Reference yield:

: 1353667-07-8
((3aR,4R,6S,6aS)-6-((E)-5-(benzyloxy)pent-2-enyl)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl acetate

: 1353667-15-8
C₂₀H₂₈O₄

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate / ethyl acetate / 1.5 h

2: lithium hydroxide pentahydrate; water / tetrahydrofuran / 4 h / 0 - 20 °C

3: tetrachloromethane; sodium hydrogencarbonate; triphenylphosphine / 48 h / Reflux

4: ammonia; lithium; ferric nitrate / 2 h / -40 °C

With tetrachloromethane; palladium 10% on activated carbon; lithium hydroxide pentahydrate; ammonia; water; hydrogen; lithium; sodium hydrogencarbonate; ferric nitrate; triphenylphosphine; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.tetlet.2011.10.117

Reference yield:

: 174392-13-3
3-(5-O-acetyl-2,3-O-isopropylidene-β-D-ribofuranosyl)prop-1-ene

: 1353667-15-8
C₂₀H₂₈O₄

Guidance literature:: Multi-step reaction with 6 steps

1: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / 1,4-dioxane; water / 8 h / 20 °C

2: potassium hexamethylsilazane / tetrahydrofuran / 1.5 h / 78 °C

3: palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate / ethyl acetate / 1.5 h

4: lithium hydroxide pentahydrate; water / tetrahydrofuran / 4 h / 0 - 20 °C

5: tetrachloromethane; sodium hydrogencarbonate; triphenylphosphine / 48 h / Reflux

6: ammonia; lithium; ferric nitrate / 2 h / -40 °C

With 2,6-dimethylpyridine; tetrachloromethane; sodium periodate; osmium(VIII) oxide; palladium 10% on activated carbon; lithium hydroxide pentahydrate; ammonia; water; hydrogen; lithium; potassium hexamethylsilazane; sodium hydrogencarbonate; ferric nitrate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; water; ethyl acetate; 2: Julia Olefin synthesis;
DOI:10.1016/j.tetlet.2011.10.117