C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂

Base Information

Chemical Name:C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂
CAS No.:1295580-58-3
Molecular Formula:C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂
Molecular Weight:875.166
Hs Code.:

C<sub>6</sub>H<sub>15</sub>N*C<sub>27</sub>H<sub>30</sub>ClN<sub>7</sub>O<sub>14</sub>P<sub>2</sub>

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Chemical Property of C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂

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Technology Process of C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂

There total 3 articles about C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1018828-95-9
C₆H₁₅N*C₂₁H₂₆BrN₇O₁₄P₂

: 1679-18-1
4-Chlorophenylboronic acid

: 15715-58-9
triethylamine carbonate

: 1295580-58-3
C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂

Guidance literature:: C₆H₁₅N*C₂₁H₂₆BrN₇O₁₄P₂; 4-Chlorophenylboronic acid; With potassium carbonate; tris(4,6-dimethyl-3-sulfonatophenyl)phosphine trisodium salt hydrate; In water; at 40 ℃; for 0.583333h; Inert atmosphere;

triethylamine carbonate;
DOI:10.1021/jm1013852

Reference yield:

: 15715-58-9
triethylamine carbonate

: 1295580-58-3
C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / water / 1.75 h / 20 °C / pH 4 / aq. acetate buffer

2: potassium carbonate; tris(4,6-dimethyl-3-sulfonatophenyl)phosphine trisodium salt hydrate / water / 0.58 h / 40 °C / Inert atmosphere

With bromine; potassium carbonate; tris(4,6-dimethyl-3-sulfonatophenyl)phosphine trisodium salt hydrate; In water; 2: Suzuki coupling;
DOI:10.1021/jm1013852

Reference yield:

: 53-84-9,66844-06-2
NAD

: 1295580-58-3
C₆H₁₅N*C₂₇H₃₀ClN₇O₁₄P₂

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / water / 1.75 h / 20 °C / pH 4 / aq. acetate buffer

2: potassium carbonate; tris(4,6-dimethyl-3-sulfonatophenyl)phosphine trisodium salt hydrate / water / 0.58 h / 40 °C / Inert atmosphere

With bromine; potassium carbonate; tris(4,6-dimethyl-3-sulfonatophenyl)phosphine trisodium salt hydrate; In water; 2: Suzuki coupling;
DOI:10.1021/jm1013852