Technology Process of C19H29N
There total 4 articles about C19H29N which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1-methanesulfonyl-oct-1-ene;
With
bis(cyclopentadienyl)titanium dichloride; magnesium; triethyl phosphite;
In
tetrahydrofuran;
at 10 ℃;
for 0.416667h;
Molecular sieve;
Inert atmosphere;
N-(buta-2,3-dienyl)-N-methylaniline;
In
tetrahydrofuran;
at 10 ℃;
for 3h;
optical yield given as %de;
regioselective reaction;
Molecular sieve;
Inert atmosphere;
DOI:10.1039/c1cc14765j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium peroxymonosulfate
2.1: bis(cyclopentadienyl)titanium dichloride; magnesium; triethyl phosphite / tetrahydrofuran / 0.42 h / 10 °C / Molecular sieve; Inert atmosphere
2.2: 3 h / 10 °C / Molecular sieve; Inert atmosphere
With
bis(cyclopentadienyl)titanium dichloride; potassium peroxymonosulfate; magnesium; triethyl phosphite;
In
tetrahydrofuran;
DOI:10.1039/c1cc14765j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: diisopropylamine; copper(I) bromide
2.1: bis(cyclopentadienyl)titanium dichloride; magnesium; triethyl phosphite / tetrahydrofuran / 0.42 h / 10 °C / Molecular sieve; Inert atmosphere
2.2: 3 h / 10 °C / Molecular sieve; Inert atmosphere
With
bis(cyclopentadienyl)titanium dichloride; magnesium; diisopropylamine; copper(I) bromide; triethyl phosphite;
In
tetrahydrofuran;
DOI:10.1039/c1cc14765j
