[(κ2-bis(1-phenyl-imidazol-2-yl)disulfide)CoCl2]*CH2Cl2

Base Information

Chemical Name:[(κ2-bis(1-phenyl-imidazol-2-yl)disulfide)CoCl2]*CH2Cl2
CAS No.:958292-20-1
Molecular Formula:CH₂Cl₂*C₁₈H₁₄Cl₂CoN₄S₂
Molecular Weight:565.3
Hs Code.:

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Chemical Property of [(κ2-bis(1-phenyl-imidazol-2-yl)disulfide)CoCl2]*CH2Cl2

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Technology Process of [(κ2-bis(1-phenyl-imidazol-2-yl)disulfide)CoCl2]*CH2Cl2

There total 2 articles about [(κ2-bis(1-phenyl-imidazol-2-yl)disulfide)CoCl2]*CH2Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 75-09-2
dichloromethane

: 30192-83-7
(1-phenyl-imidazol-2-yl)disulfide

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 958292-20-1
[(κ2-bis(1-phenyl-imidazol-2-yl)disulfide)CoCl2]*CH2Cl2

Guidance literature:: In dichloromethane; (N2); using Schlenk techniques; addn. of soln. of bis(1-phenyl-imidazol-2-yl)disulfide in CH2Cl2 to slurry of CoCl2 in CH2Cl2; stirring for 18 h; filtration, removal of volatile components from filtrate in vac., extn. with CH2Cl2; cooling at -35°C for 2 ds; crystn., drying in vac.; elem. anal.;
DOI:10.1021/ic701228y

Reference yield:

: 17452-09-4
2-mercapto-1-phenylimidazole

: 958292-05-2
[(κ2-bis(1-tert-butyl-imidazol-2-yl)disulfide)CoCl2]

: 958292-24-5
[(κ2-(phenyl)C3H2N2SSC3H2N2(tert-butyl))CoCl2]

: 958292-20-1
[(κ2-bis(1-phenyl-imidazol-2-yl)disulfide)CoCl2]*CH2Cl2

Guidance literature:: In chloroform-d1; byproducts: 1-tert-butyl-imidazole-2-thione; (N2); using Schlenk techniques; addn. of soln. of CoCl2(bis(1-tert-butyl-imidazol-2-yl)disulfide in CDCl3 to soln. of 1-phenyl-imidazole-2-thione in CDCl3 for 20 min; monitoring by NMR;
DOI:10.1021/ic701228y

Reference yield:

: 958292-05-2
[(κ2-bis(1-tert-butyl-imidazol-2-yl)disulfide)CoCl2]

: 958292-20-1
[(κ2-bis(1-phenyl-imidazol-2-yl)disulfide)CoCl2]*CH2Cl2

: 958292-24-5
[(κ2-(phenyl)C3H2N2SSC3H2N2(tert-butyl))CoCl2]

Guidance literature:: With Cp₂Fe; In chloroform-d1; (N2); using Schlenk techniques; addn. of soln. of CoCl2(bis(1-tert-butyl-imidazol-2-yl)disulfide) (containing Cp2Fe) in CDCl3 to soln. of CoCl2(bis(1-phenyl-imidazol-2-yl)disulfide) in CDCl3; transferring to NMR tube; standing for 24 h; monitoring by NMR; Kinetics;
DOI:10.1021/ic701228y