HCSi(CH₃)2NHC₆H₄CH₃(Si(CH₃)2NC₆H₄CH₃)2AlCH₃

Base Information

• Chemical Name: HCSi(CH₃)2NHC₆H₄CH₃(Si(CH₃)2NC₆H₄CH₃)2AlCH₃
• CAS No.: 958228-40-5
• Molecular Formula: C₂₉H₄₄AlN₃Si₃
• Molecular Weight: 545.926
• Mol file: 958228-40-5.mol

Synonyms:

Chemical Property of HCSi(CH₃)2NHC₆H₄CH₃(Si(CH₃)2NC₆H₄CH₃)2AlCH₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HCSi(CH₃)2NHC₆H₄CH₃(Si(CH₃)2NC₆H₄CH₃)2AlCH₃

There total 1 articles about HCSi(CH₃)2NHC₆H₄CH₃(Si(CH₃)2NC₆H₄CH₃)2AlCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

aluminium trichloride (7446-70-0) + CH[(CH3)2SiNH(p-tolyl)]3 (156053-42-8) → HCSi(CH3)2NHC6H4CH3(Si(CH3)2NC6H4CH3)2AlCH3 (958228-40-5)

Guidance literature:

In hexane; toluene; byproducts: CH4; (Ar or N2; Schlenk) 1 equiv of AlCl3 in hexane was added to a soln. of amine-compound in toluene at -30°C, the mixt. was allowed to warm to room temp. while being stirred for 12 h which the soln. was slowly heated to reflux for 4 h, cooled; evapd. to dryness under vac., extd. with hexane, kept at -30°C for ca. 2 months;

DOI:10.1021/om700587w

upstream raw materials:

aluminium trichloride

CH[(CH₃)2SiNH(p-tolyl)]3