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4-Methyl-cyclohex-3-enecarboxylic acid 2-methoxy-3-methyl-cyclopent-2-enyl ester

Base Information Edit
  • Chemical Name:4-Methyl-cyclohex-3-enecarboxylic acid 2-methoxy-3-methyl-cyclopent-2-enyl ester
  • CAS No.:100231-42-3
  • Molecular Formula:C15H22O3
  • Molecular Weight:250.338
  • Hs Code.:
  • Mol file:100231-42-3.mol
4-Methyl-cyclohex-3-enecarboxylic acid 2-methoxy-3-methyl-cyclopent-2-enyl ester

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 4-Methyl-cyclohex-3-enecarboxylic acid 2-methoxy-3-methyl-cyclopent-2-enyl ester Edit
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Technology Process of 4-Methyl-cyclohex-3-enecarboxylic acid 2-methoxy-3-methyl-cyclopent-2-enyl ester

There total 2 articles about 4-Methyl-cyclohex-3-enecarboxylic acid 2-methoxy-3-methyl-cyclopent-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 8.11 g / DIBAL / diethyl ether; hexane / 4 h / 0 °C
2: 96 percent / DMAP, DCC / CH2Cl2 / 5 h / Ambient temperature
With dmap; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo00354a018
Guidance literature:
Multi-step reaction with 5 steps
2: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 6 h
3: 1.2 g / 1 h
4: 1.) LiAlH4, 2.) Et3N / 1.) ether, 12 h, 2.) CH2Cl2, -10 deg C, 20 min
5: zinc-copper couple, NaI, HMPA / 1,2-dimethoxy-ethane / 48 h / 83 °C
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; zinc copper; tetrabutyl ammonium fluoride; triethylamine; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1021/jo00354a018
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