1,2-Dimethylacenaphthene-1,2-diol

Base Information

Chemical Name:1,2-Dimethylacenaphthene-1,2-diol
CAS No.:92495-72-2
Molecular Formula:C₁₄H₁₄O₂
Molecular Weight:214.264
Hs Code.:
European Community (EC) Number:661-058-6
Nikkaji Number:J679.938H

Synonyms:1,2-Dimethylacenaphthene-1,2-diol;SCHEMBL14262737;AKOS024340968;(z)-1,2-dihydroxy-1,2-dimethylacenaphthene;1,2-DIMETHYL-1,2-DIHYDROACENAPHTHYLENE-1,2-DIOL

Suppliers and Price of 1,2-Dimethylacenaphthene-1,2-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Dimethylacenaphthene-1,2-diol

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:214.099379685
Heavy Atom Count:16
Complexity:275

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(C2=CC=CC3=C2C(=CC=C3)C1(C)O)O

Technology Process of 1,2-Dimethylacenaphthene-1,2-diol

There total 2 articles about 1,2-Dimethylacenaphthene-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917-64-6
methyl magnesium iodide

: 82-86-0
acenaphthene quinone

: 6566-38-7
cis-1,2-dihydroxy-1,2-dimethyl-1,2-dihydroacenaphthalene

: 6566-38-7,6566-39-8,89986-88-9,92495-72-2
trans-1,2-dihydroxy-1,2-dimethyl-1,2-dihydroacenaphthalene

Guidance literature:: With diethyl ether;

Reference yield:

: 6566-38-7,6566-39-8,89986-88-9,92495-72-2
trans-1,2-Dimethyl-acenaphthendiol-1,2

Guidance literature:: Acenaphthenchinon, Methylmagnesiumiodid, Ae., erwaermen; neben d. cis-Isomeren;
DOI:10.1139/v66-196

Reference yield:

: 92495-72-2
1,2-dihydroxy-1,2-dimethyl-1,2-dihydroacenaphthalene

: 52477-75-5
fluoranthenedinitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / acetic anhydride / toluene / 17 h / Heating

2: 91 percent / dichlorodicyanobenzoquinone / dioxane / 17 h / Heating

With acetic anhydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; toluene;
DOI:10.1246/cl.1998.423