benzyl alcohol-d1

Base Information

• Chemical Name: benzyl alcohol-d1
• CAS No.: 52949-66-3
• Molecular Formula: C₇H₈O
• Molecular Weight: 109.132

Synonyms:

Chemical Property of benzyl alcohol-d1

Chemical Property:

Purity/Quality:

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Technology Process of benzyl alcohol-d1

There total 18 articles about benzyl alcohol-d1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzaldehyde (100-52-7) → benzyl alcohol-d1 (3481-15-0,4181-90-2,52949-66-3,4546-45-6)

Guidance literature:

With lithium aluminium deuteride; In diethyl ether; for 3h; Heating;

DOI:10.1021/ja00076a017

Reference yield: 95.0%

benzoic acid methyl ester (93-58-3,5705-52-2,80226-58-0) → benzyl alcohol-d1 (3481-15-0,4181-90-2,52949-66-3,4546-45-6)

Guidance literature:

With sodium borodeuteride; ethane-1,2-dithiol; In tetrahydrofuran; at 80 ℃;

DOI:10.1039/c8ob01558a

Reference yield: 48.0%

trans-Dihydro-3-phenyl-5-(phenylmethyl)-6-heptyl-1,2,4,5-trioxazine (122744-71-2) → benzyl alcohol-d1 (3481-15-0,4181-90-2,52949-66-3,4546-45-6) + α-<2H1>-N-Benzyl-N-octylhydroxylamine

Guidance literature:

With lithium aluminium deuteride; In diethyl ether; for 18h; Ambient temperature;

DOI:10.1021/jo00034a018

upstream raw materials:

ethyl-(α,α-dideuterio-benzyl)-ether

propyl sodium

benzaldehyde

benzoic acid methyl ester

Downstream raw materials:

(chloromethyl-d)benzene

4-nitro-benzoic acid-(α-deuterio-benzyl ester)

C₁₅H₂₂⁽²⁾HN₂OP

exo-3,4,6-tri-O-acetyl-1,2-O-(1-benzyloxy-α-d-ethylidene)-β-D-mannopyranose

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