N-phenyl-2,3,4,5,6-pentadeueriobenzamide

Base Information

• Chemical Name: N-phenyl-2,3,4,5,6-pentadeueriobenzamide
• CAS No.: 1415308-47-2
• Molecular Formula: C₁₃H₁₁NO
• Molecular Weight: 202.197
• Mol file: 1415308-47-2.mol

Synonyms:

Chemical Property of N-phenyl-2,3,4,5,6-pentadeueriobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-phenyl-2,3,4,5,6-pentadeueriobenzamide

There total 1 articles about N-phenyl-2,3,4,5,6-pentadeueriobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoyl chloride-d5 (43019-90-5) + aniline (62-53-3) → N-phenyl-2,3,4,5,6-pentadeueriobenzamide (1415308-47-2)

Guidance literature:

In dichloromethane; at 0 ℃; for 4h;

DOI:10.1039/c2ob26668g

Reference yield:

N-phenyl benzoyl amide (93-98-1,5705-51-1) + N-phenyl-2,3,4,5,6-pentadeueriobenzamide (1415308-47-2) + diphenyl acetylene (501-65-5) → C27H15(2)H4NO (1415308-48-3) + 2,3,4-triphenylisoquinolin-1(2H)-one (14959-72-9)

Guidance literature:

With copper(II) choride dihydrate; palladium diacetate; sodium bromide; potassium hydroxide; In N,N-dimethyl-formamide; at 120 ℃; for 6h; Overall yield = 26 %; Overall yield = 19 mg;

DOI:10.1039/c2ob26668g

upstream raw materials:

benzoyl chloride-d5

aniline

Downstream raw materials:

C₂₇H₁₅⁽²⁾H₄NO

2,3,4-triphenylisoquinolin-1(2H)-one