Technology Process of C15H14N4
There total 5 articles about C15H14N4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / -78 °C
1.2: -78 - 20 °C
2.1: Reflux
3.1: copper(l) iodide / N,N-dimethyl acetamide / 150 °C
4.1: hydrazine hydrate / ethanol / Reflux
With
copper(l) iodide; hydrazine hydrate; lithium diisopropyl amide;
In
ethanol; N,N-dimethyl acetamide;
DOI:10.1039/c2md20239e
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1,1'-carbonyldiimidazole; triethylamine / dichloromethane / 20 °C
2.1: lithium diisopropyl amide / -78 °C
2.2: -78 - 20 °C
3.1: Reflux
4.1: copper(l) iodide / N,N-dimethyl acetamide / 150 °C
5.1: hydrazine hydrate / ethanol / Reflux
With
copper(l) iodide; hydrazine hydrate; triethylamine; 1,1'-carbonyldiimidazole; lithium diisopropyl amide;
In
ethanol; dichloromethane; N,N-dimethyl acetamide;
DOI:10.1039/c2md20239e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Reflux
2: copper(l) iodide / N,N-dimethyl acetamide / 150 °C
3: hydrazine hydrate / ethanol / Reflux
With
copper(l) iodide; hydrazine hydrate;
In
ethanol; N,N-dimethyl acetamide;
DOI:10.1039/c2md20239e