(S)-cyclohexyl 2-[benzyl(methyl)amino]propanoate

Base Information

Chemical Name:(S)-cyclohexyl 2-[benzyl(methyl)amino]propanoate
CAS No.:1353757-57-9
Molecular Formula:C₁₇H₂₅NO₂
Molecular Weight:275.391
Hs Code.:

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Chemical Property of (S)-cyclohexyl 2-[benzyl(methyl)amino]propanoate

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Technology Process of (S)-cyclohexyl 2-[benzyl(methyl)amino]propanoate

There total 5 articles about (S)-cyclohexyl 2-[benzyl(methyl)amino]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1353757-82-0
C₁₆H₂₃NO₂

: 1353757-57-9
(S)-cyclohexyl 2-[benzyl(methyl)amino]propanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; water; for 12h;
DOI:10.1039/c1ob06074k

Reference yield:

: C₁₆H₂₁NO₂

: 1353757-57-9
(S)-cyclohexyl 2-[benzyl(methyl)amino]propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 12 h / 0 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol; water / 12 h

With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; In methanol; ethanol; water;
DOI:10.1039/c1ob06074k

Reference yield:

: Z-L-Ala cyclohexyl ester

: 1353757-57-9
(S)-cyclohexyl 2-[benzyl(methyl)amino]propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C

2: trimethyl orthoformate / 48 h / 20 °C / Inert atmosphere

3: sodium tetrahydroborate / methanol / 12 h / 0 - 20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / ethanol; water / 12 h

With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; trimethyl orthoformate; In methanol; ethanol; water; ethyl acetate;
DOI:10.1039/c1ob06074k