racem.-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane

Base Information

Chemical Name:racem.-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane
CAS No.:103402-11-5
Molecular Formula:C₃₆H₄₂O₁₀S₂
Molecular Weight:698.855
Hs Code.:

<i>racem.</i>-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of racem.-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane

Chemical Property:

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Technology Process of racem.-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane

There total 12 articles about racem.-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5507-27-7
3,4-dimethoxybenzylidenesuccinic acid

: 103402-11-5
meso-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane

Guidance literature:: Multi-step reaction with 6 steps

1: methanol. H₂SO₄

2: sodium ethylate; ethanol / anschliessend Erwaermen unter Zusatz von H₂O

3: Raney nickel; aluminium; aqueous NaOH / 90 °C / Hydrogenation

4: methanol; acetone; diethyl ether

5: LiAlH₄; THF

With tetrahydrofuran; methanol; sodium hydroxide; lithium aluminium tetrahydride; diethyl ether; ethanol; sulfuric acid; sodium ethanolate; nickel; acetone; aluminium;
DOI:10.1021/ja01571a054

Reference yield:

: 5507-27-7
3,4-dimethoxybenzylidenesuccinic acid

: 103402-11-5
racem.-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane

Guidance literature:: Multi-step reaction with 6 steps

1: methanol. H₂SO₄

2: sodium ethylate; ethanol / anschliessend Erwaermen unter Zusatz von H₂O

3: Raney nickel; aluminium; aqueous NaOH / 90 °C / Hydrogenation

4: acetic acid anhydride

5: LiAlH₄; THF

With tetrahydrofuran; sodium hydroxide; lithium aluminium tetrahydride; ethanol; sulfuric acid; sodium ethanolate; acetic anhydride; nickel; aluminium;
DOI:10.1021/ja01571a054

Reference yield:

: 42923-56-8
veratrylidene-succinic acid dimethyl ester

: 103402-11-5
meso-1,4-bis-(toluene-4-sulfonyloxy)-2,3-diveratryl-butane

Guidance literature:: Multi-step reaction with 5 steps

1: sodium ethylate; ethanol / anschliessend Erwaermen unter Zusatz von H₂O

2: Raney nickel; aluminium; aqueous NaOH / 90 °C / Hydrogenation

3: methanol; acetone; diethyl ether

4: LiAlH₄; THF

With tetrahydrofuran; methanol; sodium hydroxide; lithium aluminium tetrahydride; diethyl ether; ethanol; sodium ethanolate; nickel; acetone; aluminium;
DOI:10.1021/ja01571a054