1'-(diphenylphosphino)-1-ferrocenecarboxylate

Base Information

Chemical Name:1'-(diphenylphosphino)-1-ferrocenecarboxylate
CAS No.:1213267-05-0
Molecular Formula:C₂₆H₂₇FeO₂PSn
Molecular Weight:577.03
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1'-(diphenylphosphino)-1-ferrocenecarboxylate

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Technology Process of 1'-(diphenylphosphino)-1-ferrocenecarboxylate

There total 1 articles about 1'-(diphenylphosphino)-1-ferrocenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 173346-69-5
1′-(diphenylphosphino)ferrocene-1-carboxylic acid

: 1066-45-1
trimethyltin(IV)chloride

: 865-47-4
potassium tert-butylate

: 1213267-05-0
1'-(diphenylphosphino)-1-ferrocenecarboxylate

Guidance literature:: In dichloromethane; byproducts: KCl; under Ar; tBuOK added to soln. of Fc deriv. in CH2Cl2; stirred at room temp. for 30 min; to K salt ppt. added Me3SnCl in CH2Cl2; stirred overnight, react. mixt. diluted with pentane; allowed to stand for 30 min; filtered through celite; evapd.; crystd. from hot heptane or from ethyl acetate-hexane; elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.042