[tris(diisopropylphosphino)borate]CoCl

Base Information

Chemical Name:[tris(diisopropylphosphino)borate]CoCl
CAS No.:579444-63-6
Molecular Formula:C₂₇H₅₃BClCoP₃
Molecular Weight:575.896
Hs Code.:

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Chemical Property of [tris(diisopropylphosphino)borate]CoCl

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Technology Process of [tris(diisopropylphosphino)borate]CoCl

There total 2 articles about [tris(diisopropylphosphino)borate]CoCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 579444-61-4
[tris(diisopropylphosphino)borate]thallium

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 579444-63-6
[tris(diisopropylphosphino)borate]CoCl

Guidance literature:: In tetrahydrofuran; N2; addn. of THF soln. of the borate to stirring THF suspn. of FeCl2 at room temp., stirring for 2 h; filtration (Celite), evapn. to dryness in vac., dissolving the solid in benzene, filtration again, crystn. by slow evapn. of benzene soln.; elem. anal.;
DOI:10.1021/ic0343096

Reference yield: 87.0%

: 627090-51-1
[Li(tetrahydrofuran)PhB(CH₂P(i)Pr₂)3]

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 579444-63-6
[tris(diisopropylphosphino)borate]CoCl

Guidance literature:: In tetrahydrofuran; at -30 ℃; for 4h; Glovebox; Inert atmosphere;
DOI:10.1021/acs.organomet.8b00635

Reference yield: 99.0%

: 579444-63-6
[tris(diisopropylphosphino)borate]CoCl

: 201230-82-2
carbon monoxide

: 579444-68-1
[tris(diisopropylphosphino)borate]CoCl(carbon monoxide)

Guidance literature:: In benzene; sparging benzene soln. of the complex with CO at room temp. with stirring for 1 min, stirring for 0.5 h; evapn. to dryness in vac.; elem. anal.;
DOI:10.1021/ic0343096