6β--estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride

Base Information

Chemical Name:6β--estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride
CAS No.:107612-24-8
Molecular Formula:C₃₁H₄₁NO₃*ClH
Molecular Weight:512.132
Hs Code.:

6β-<p-(2-Diethylaminoethoxy)phenyl>-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6β--estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride

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Technology Process of 6β--estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride

There total 3 articles about 6β--estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107612-20-4
6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether

: 107612-24-8
6β--estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 0.205 g / H₂, diethylamine / Raney nickel / methanol / 2 h / Ambient temperature

2: 0.6 g / K₂CO₃ / dimethylsulfoxide / 12 h / Ambient temperature

With hydrogen; potassium carbonate; diethylamine; nickel; In methanol; dimethyl sulfoxide;

Reference yield:

: 107612-18-0,107612-19-1
(8R,9S,13S,14S,17S)-6-(4-Benzyloxy-phenyl)-3-methoxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthrene-6,17-diol

: 107612-24-8
6β--estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: conc. HCl / methanol / 0.5 h / Heating

2: 0.205 g / H₂, diethylamine / Raney nickel / methanol / 2 h / Ambient temperature

3: 0.6 g / K₂CO₃ / dimethylsulfoxide / 12 h / Ambient temperature

With hydrogenchloride; hydrogen; potassium carbonate; diethylamine; nickel; In methanol; dimethyl sulfoxide;